化工社化工社 化学情報印刷レポート · 研究参考用
1,2-Dibromopropane → 1,3-Bis(4'-methoxyphenyl)-2-imino-4-methyl-imidazolidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Dibromopropane | HCID 6553 | — |
| 反応物 | P-Anisidine | HCID 7732 | — |
| 反応物 | 1,2-Bis(4'-methoxyphenyl-amino)-propane | HCID 20512439 | — |
| 生成物 | 1,3-Bis(4'-methoxyphenyl)-2-imino-4-methyl-imidazolidine | HCID 13881460 | 32.7% |
反応手順
1,2-Bis(4'-methoxyphenyl-amino)-propane, applied as starting substance, is obtained with a yield of 32.7% by reacting 4-methoxyaniline with 1,2-dibromopropane as described by McKay and Tarlton (loc. cit.). The compound melts at 82°-84° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04284642 |
| 出典データセット | uspto-grants-1981_08 |
| ORD ID | ord-de8e557985ee4d19975c5493df9169d8 |
| 出典メモ | uspto-grants-1981_08 |