3-(1,1-Dimethyloctyl)phenol → 3-(2-Methyloctan-2-yl)phenol

HRID 894910

反応式

HRID 894910 の反応式
[OH:1][C:2]1[CH:3]=[C:4]([C:8]([CH3:17])([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15]C)[CH3:9])[CH:5]=[CH:6][CH:7]=1.C(OC1C=CC=C(C(C)(C)C=CCCCCC)C=1)C1C=CC=CC=1>>[OH:1][C:2]1[CH:3]=[C:4]([C:8]([CH3:17])([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])[CH3:9])[CH:5]=[CH:6][CH:7]=1

参加物

3

反応物 2

HCID 204969203-(1,1-Dimethyloctyl)phenolHCID 542462321-Benzyloxy-3-(1,1-dimethyloct-2-enyl)benzene

生成物 1

HCID 127881863-(2-Methyloctan-2-yl)phenol

実験手順

In like manner, 2-(3-hydroxyphenyl)-2-methylnonane is prepared in 82% (7.8 g.) yield from 13.0 g. (0.0406 mol.) of 1-benzyloxy-3-(1,1-dimethyl-oct-2-enyl)benzene. It is obtained as an oil having the characteristics:

後処理

  1. customyield from 13.0 g
  2. customIt is obtained as an oil

出典と根拠

ORDレコード
ord-3280d7f1a13e4d09bb779a3edf0c3d3e
出典データセット
uspto-grants-1981_08
特許番号
US04284829

関連ノート

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