Hydrazine → HCID 136359185、化合物
反応式
[CH3:1][C:2]12[CH2:12][CH2:11][CH:5]([C:6](=[N:9][OH:10])[C:7]1=O)[CH:4]([CH3:13])[O:3]2.[NH2:14][NH2:15]>C(O)C>[CH3:1][C:2]12[CH2:12][CH2:11][CH:5]([C:6](=[N:9][OH:10])[C:7]1=[N:14][NH2:15])[CH:4]([CH3:13])[O:3]2参加物
4
実験手順
A mixture of 1.83 g. (0.01 mole) 1,3-dimethyl-2-oxabicyclo[2,2,2]octan-5,6-dione-5-oxime and 0.35 ml. (0.011 mole) anhydrous hydrazine (98%) in 25 ml. absolute ethanol is refluxed under nitrogen at a bath temperature of 80° C. for 1 hour. Evaporation of the solvent gives 1,3-dimethyl-2-oxa-bicyclo[2,2,2]octan-5,6-dione-5-oxime-6-hydrazone.
後処理
- additionA mixture of 1.83 g
- customEvaporation of the solvent
出典と根拠
- ORDレコード
- ord-777b7eee3d114927a507276c06dc3c71
- 出典データセット
- uspto-grants-1981_08
- 特許番号
- US04285944
反応ノート
読み込み中…