Methanol → HCID 59896206、化合物

反応式

[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([OH:10])=[O:9])[NH2:7].[CH3:11]O>>[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([O:10][CH3:11])=[O:9])[NH2:7]

参加物

反応物 2

HCID 887Methanol

HCID 99558S-(2-Aminoethyl)-L-cysteine

生成物 1

HCID 59896206HCID 59896206、化合物

実験手順

A 10 g (50 mmol) sample of S-(2-aminoethyl)-L-cysteine was dissolved in 400 mL of methanol. Into this cooled solution was bubbled in anhydrous HCl for 30 minutes. After stirring at room temperature overnight, the solution was concentrated to afford 12.7 g of the title compound.

後処理

customInto this cooled solution was bubbled in anhydrous HCl for 30 minutes
concentrationthe solution was concentrated

出典と根拠

ORDレコード: ord-0086953fef694a4197e1077e07363b4c
出典データセット: uspto-grants-2005_07
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06914158B2

反応ノート

読み込み中…

参加物