化工社化工社 化学情報印刷レポート · 研究参考用
2-Methyl-6-nitrophenol → 6-Amino-o-cresol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methyl-6-nitrophenol | HCID 83103 | — |
| 反応物 | 2-Amino-6-chlorophenol | HCID 6486025 | — |
| 生成物 | 6-Amino-o-cresol | HCID 413657 | — |
反応手順
2-amino-6-methylphenol was prepared from 2-methyl-6-nitrophenol (0.500 g, 3.26 mmol) in a manner similar to that described for 2-amino-6-chlorophenol. The compound was formed as a black solid (0.030 g, 8%). RP-HPLC (25 to 100% CH3CN in 0.1 N aqueous ammonium acetate over 10 min at 1 mL/min using a Hypersil HS C18, 100 Å, 5 μm, 250×4.6 mm column) tr=5.78 min., 86%; m/z 123 (MH+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06921763B2 |
| 出典データセット | uspto-grants-2005_07 |
| ORD ID | ord-746ca0b39d004ca6994778eb64e4c805 |
| 出典メモ | uspto-grants-2005_07 |