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Piperazine → n,n'-Bis-((e)-3-(2-methoxyphenyl)-2-propenyl)piperazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Piperazine | HCID 4837 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 2-Methoxy-cinnamylalcohol | HCID 53401658 | — |
| 生成物 | n,n'-Bis-((e)-3-(2-methoxyphenyl)-2-propenyl)piperazine | HCID 19694161 | — |
反応手順
2-Methoxy-cinnamylalcohol (1.44 g) was chlorinated using thionylchloride. Subsequently, reaction with piperazine and other treatments were performed as described in Preparation Example 2, to thereby obtain 314 mg of a salt as colorless prisms.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05723465 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-d2aea31453084c8dba037f866c0833b5 |
| 出典メモ | uspto-grants-1998_03 |