5-Methoxyindole → [(5-Methoxy-1H-indol-3-yl)-phenylmethyl]-dimethylamine

反応式

[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][CH:11]=1)[NH:8][CH:7]=[CH:6]2.[Cl-].[CH:13](=[N+:20]([CH3:22])[CH3:21])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][CH:11]=1)[NH:8][CH:7]=[C:6]2[CH:13]([N:20]([CH3:22])[CH3:21])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

参加物

反応物 2

HCID 138725-Methoxyindole

HCID 11073839Methanaminium, N-methyl-N-(phenylmethylene)-, chloride

生成物 1

HCID 9814267[(5-Methoxy-1H-indol-3-yl)-phenylmethyl]-dimethylamine

実験手順

The preparation was carried out in accordance with general synthesis instructions 4 from 5-methoxy-1H-indole and benzylidene-dimethyl-ammonium chloride, which had been prepared in accordance with example 1.

後処理

customhad been prepared in accordance with example 1

出典と根拠

ORDレコード: ord-534b098f3a2c49f69c538b07cabcb376
出典データセット: uspto-grants-2006_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07091220B2

反応ノート

読み込み中…