5-Chloroindole → [(5-Chloro-1H-indol-3-yl)-phenylmethyl]-dimethylamine

反応式

[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[NH:7][CH:6]=[CH:5]2.[Cl-].[CH:12](=[N+:19]([CH3:21])[CH3:20])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[NH:7][CH:6]=[C:5]2[CH:12]([N:19]([CH3:21])[CH3:20])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

参加物

反応物 2

HCID 871105-Chloroindole

HCID 11073839Methanaminium, N-methyl-N-(phenylmethylene)-, chloride

生成物 1

HCID 9814391[(5-Chloro-1H-indol-3-yl)-phenylmethyl]-dimethylamine

実験手順

The preparation was carried out in accordance with general synthesis instructions 4 from 5-chloro-1H-indole and benzylidene-dimethyl-ammonium chloride, which had been prepared in accordance with example 1.

後処理

customhad been prepared in accordance with example 1

出典と根拠

ORDレコード: ord-15cb9b2285214b0198c4d91d20a3fcb1
出典データセット: uspto-grants-2006_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07091220B2

反応ノート

読み込み中…