化工社化工社 化学情報印刷レポート · 研究参考用
Methyl 3-(bromomethyl)benzoate → 3-(4'-Methoxy-biphenyl-4-yloxymethyl)-benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 3-(bromomethyl)benzoate | HCID 517981 | — |
| 反応物 | 4-Hydroxy-4'-methoxybiphenyl | HCID 11030839 | — |
| 生成物 | 3-(4'-Methoxy-biphenyl-4-yloxymethyl)-benzoic acid | HCID 11359559 | — |
反応手順
3-(4′-Methoxy-biphenyl-4-yloxymethyl)-benzoic acid was prepared using general procedure A from 4-hydroxy-4′-methoxybiphenyl (available from TCI America, Portland, Oreg.) and 3-(bromomethyl)benzoic acid methyl ester (available from Lancaster Synthesis Ltd., Morcambe, Lancashire, UK). Yield: 73 mg. Mass spectrum (ES) MH+=335.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07355049B2 |
| 出典データセット | uspto-grants-2008_04 |
| ORD ID | ord-64bdf561bd264f2594643cf921d70772 |
| 出典メモ | uspto-grants-2008_04 |