1-Methylindole → Dimethyl-[(1-methyl-1H-indol-3-yl)-phenylmethyl]-amine

反応式

[CH3:1][N:2]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3]1.[Cl-].[CH:12](=[N+:19]([CH3:21])[CH3:20])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[CH3:20][N:19]([CH3:21])[CH:12]([C:4]1[C:5]2[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=2)[N:2]([CH3:1])[CH:3]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

参加物

反応物 2

HCID 117811-Methylindole

HCID 11073839Methanaminium, N-methyl-N-(phenylmethylene)-, chloride

生成物 1

HCID 9795272Dimethyl-[(1-methyl-1H-indol-3-yl)-phenylmethyl]-amine

実験手順

The preparation was carried out in accordance with general synthesis instructions 4 from 1-methyl-1H-indole and benzylidene-dimethyl-ammonium chloride, which had been prepared in accordance with example 1.

後処理

customhad been prepared in accordance with example 1

出典と根拠

ORDレコード: ord-d2c82f1e0a8e471f948109909b31a5ff
出典データセット: uspto-grants-2006_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07091220B2

反応ノート

読み込み中…