化工社化工社 化学情報印刷レポート · 研究参考用
Acetyl chloride → 1-(2-Methyl-benzylidene)-pyrrolidinium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetyl chloride | HCID 6367 | — |
| 反応物 | 2-Methylbenzaldehyde | HCID 10722 | — |
| 反応物 | Pyrrolidine | HCID 31268 | — |
| 生成物 | 1-(2-Methyl-benzylidene)-pyrrolidinium chloride | HCID 17912280 | — |
反応手順
The reaction of 8.2 ml (0.100 mol) pyrrolidine and 7.0 g (0.050 mol) 2-methylbenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 3.9 g (0.050 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 6.6 g (corresponding to 63% of the yield calculated by theory) 1-(2-methyl-benzylidene)-pyrrolidinium chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07091220B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-d745609141254580931317ff1b8db479 |
| 出典メモ | uspto-grants-2006_08 |