反応式
[CH:1]1([C:7]([O:9]C)=O)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[NH2:11][NH2:12]>CO>[CH:1]1([C:7]([NH:11][NH2:12])=[O:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1参加物
4
反応条件
- 温度
- 65 °C
実験手順
To a solution of methyl cyclohexane carboxylate (12 g, 83.9 mmol) in MeOH (50 mL) was added hydrazine (5.3 mL, 1.67 mol). The reaction mixture was heated at 65° C. overnight. The reaction mixture was cooled to room temperature and the resultant solid was collected by filtration and was dried in vacuo to give 4.0 g of cyclohexanecarboxylic acid hydrazide.
後処理
- temperatureThe reaction mixture was cooled to room temperature
- filtrationthe resultant solid was collected by filtration
- customwas dried in vacuo
出典と根拠
- ORDレコード
- ord-0f7b1b1ab58e47aa88a8b07dc365b917
- 出典データセット
- uspto-grants-2008_04
- 特許番号
- US07358242B2
関連ノート
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