化工社化工社 化学情報印刷レポート · 研究参考用
Acetyl chloride → 1-(2-Chloro-benzylidene)-piperidinium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetyl chloride | HCID 6367 | — |
| 反応物 | 2-Chlorobenzaldehyde | HCID 6996 | — |
| 反応物 | Piperidine | HCID 8082 | — |
| 生成物 | 1-(2-Chloro-benzylidene)-piperidinium chloride | HCID 17958747 | — |
反応手順
The reaction of 8.5 g (0.100 mol) piperidine and 7.0 g (0.050 mol) 2-chlorobenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 3.9 g (0.050 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 7.1 g (corresponding to 58% of the yield calculated by theory) 1-(2-chloro-benzylidene)-piperidinium chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07091220B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-b6f01e61c48544b0ba58cf7e12990b46 |
| 出典メモ | uspto-grants-2006_08 |