化工社化工社 化学情報印刷レポート · 研究参考用
Acetyl chloride → 1-(2-Methyl-benzylidene)-piperidinium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetyl chloride | HCID 6367 | — |
| 反応物 | Piperidine | HCID 8082 | — |
| 反応物 | 2-Methylbenzaldehyde | HCID 10722 | — |
| 生成物 | 1-(2-Methyl-benzylidene)-piperidinium chloride | HCID 17912257 | — |
反応手順
The reaction of 9.5 ml (0.096 mol) piperidine and 4.7 ml (0.040 mol) 2-methylbenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 2.4 ml (0.040 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 5.8 g (corresponding to 65% of the yield calculated by theory) 1-(2-methyl-benzylidene)-piperidinium chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07091220B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-00adf1ba992d4cb99f816842b438f344 |
| 出典メモ | uspto-grants-2006_08 |