化工社化工社 化学情報印刷レポート · 研究参考用
Propanenitrile, 3-(methylamino)- → N-(2-cyanoethyl)-N-methyl-2-(trifluoromethyl)benzenesulphonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Propanenitrile, 3-(methylamino)- | HCID 69656 | — |
| 反応物 | 2-Trifluoromethylbenzenesulphonyl chloride | HCID 136616 | — |
| 生成物 | N-(2-cyanoethyl)-N-methyl-2-(trifluoromethyl)benzenesulphonamide | HCID 43084128 | — |
反応手順
In operating analogously to Preparation V, starting with 2-(trifluoromethyl)benzenesulphonyl chloride and 3-(methylamino)propionitrile, the expected product is obtained as a yellow oil (yield=98%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07361687B2 |
| 出典データセット | uspto-grants-2008_04 |
| ORD ID | ord-1637b96defe1476fb9d1cdac926f88e7 |
| 出典メモ | uspto-grants-2008_04 |