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Dimethylamine → (2-Methyl-benzylidene)-dimethylammonium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylamine | HCID 674 | — |
| 反応物 | Acetyl chloride | HCID 6367 | — |
| 反応物 | 2-Methylbenzaldehyde | HCID 10722 | — |
| 生成物 | (2-Methyl-benzylidene)-dimethylammonium chloride | HCID 21985341 | — |
反応手順
The reaction of 14.0 ml (0.108 mol) dimethylamine solution and 4.6 ml (0.040 mol) 2-methylbenzaldehyde in accordance with general synthesis instructions 1 and subsequent reaction with 2.4 ml (0.040 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 5.3 g (corresponding to 73% of the yield calculated by theory) dimethyl-(2-methyl-benzylidene)-ammonium chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07091220B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-9d6a01b849784a7f99927f8025b4abe7 |
| 出典メモ | uspto-grants-2006_08 |