5-Benzyloxyindole → [(5-Benzyloxy-1H-indol-3-yl)-o-tolylmethyl]-dimethylamine

HRID 9019

反応式

HRID 9019 の反応式
[CH2:1]([O:8][C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][CH:13]=[CH:12]2)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Cl-].[CH3:19][N+:20]([CH3:29])=[CH:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][C:23]=1[CH3:28]>>[CH2:1]([O:8][C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][CH:13]=[C:12]2[CH:21]([N:20]([CH3:19])[CH3:29])[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][C:23]=1[CH3:28])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

参加物

3

反応物 2

HCID 146245-BenzyloxyindoleHCID 21985341(2-Methyl-benzylidene)-dimethylammonium chloride

生成物 1

HCID 9947572[(5-Benzyloxy-1H-indol-3-yl)-o-tolylmethyl]-dimethylamine

実験手順

The preparation was carried out in accordance with general synthesis instructions 4 from 5-benzyloxy-1H-indole and dimethyl-(2-methyl-benzylidene)-ammonium chloride, which had been prepared in accordance with example 32.

後処理

  1. customhad been prepared in accordance with example 32

出典と根拠

ORDレコード
ord-117472a0d67b480f955f6ad22ff17526
出典データセット
uspto-grants-2006_08
特許番号
US07091220B2

関連ノート

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