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Dimethylamine → 2-Methoxy-benzylidene-dimethyl-ammonium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylamine | HCID 674 | — |
| 反応物 | Acetyl chloride | HCID 6367 | — |
| 反応物 | 2-Methoxybenzaldehyde | HCID 8658 | — |
| 生成物 | 2-Methoxy-benzylidene-dimethyl-ammonium chloride | HCID 21985303 | — |
反応手順
The reaction of 17.0 ml (0.135 mol) dimethylamine solution and 6.8 g ml (0.050 mol) 2-methoxybenzaldehyde in accordance with general synthesis instructions 1 and subsequent reaction with 3.0 ml (0.050 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 4.8 g (corresponding to 48% of the yield calculated by theory) 2-methoxy-benzylidene-dimethyl-ammonium chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07091220B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-6fc688613ae646f2a32ab26807d5074f |
| 出典メモ | uspto-grants-2006_08 |