Hydrochloric Acid → 2(1-Methyl-5-pyrazolyl) amino-2-imidazoline hydrochloride

HRID 903051ノート

反応式

HRID 903051 の反応式
C([N:4]1[CH2:8][CH2:7][N:6]=[C:5]1[NH:9][C:10]1[N:14]([CH3:15])[N:13]=[CH:12][CH:11]=1)(=O)C.[ClH:16]>CO>[ClH:16].[CH3:15][N:14]1[C:10]([NH:9][C:5]2[NH:6][CH2:7][CH2:8][N:4]=2)=[CH:11][CH:12]=[N:13]1

参加物

4

反応物 2

HCID 313Hydrochloric AcidHCID 127637911-Acetyl-2(1-methyl-5-pyrazolyl)amino-2-imidazoline

生成物 1

HCID 705934332(1-Methyl-5-pyrazolyl) amino-2-imidazoline hydrochloride

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

1-Acetyl-2(1-methyl-5-pyrazolyl)amino-2-imidazoline (37.4 g.) was treated with HCl in methanol as described in Example II to give 25.9 g. product mp 204-208 which was converted to the hydrochloride salt mp 187-189.

後処理

  1. customto give 25.9 g

出典と根拠

ORDレコード
ord-2aca7c475c8d4792bcf856c18b13f756
出典データセット
uspto-grants-1980_10
特許番号
US04226773

反応ノート

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