1,3-Propanediamine → HCID 70546801、化合物

HRID 903087

反応式

HRID 903087 の反応式
C[NH:2][C:3]1[C:16]2[C:15](=[O:17])[C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[C:8](=[O:18])[C:7]=2[C:6](Br)=[CH:5][CH:4]=1.[NH2:20][CH2:21][CH2:22][CH2:23][NH2:24].[C:25]1(C)C=CC=CC=1>>[CH3:25][NH:20][C:21]1[C:16]2[C:15](=[O:17])[C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[C:8](=[O:18])[C:7]=2[C:6]([CH2:5][CH2:4][CH2:3][NH2:2])=[C:23]([NH2:24])[CH:22]=1

参加物

4

反応物 3

HCID 4281,3-PropanediamineHCID 1140TolueneHCID 314189,10-Anthracenedione, 1-bromo-4-(methylamino)-

生成物 1

HCID 70546801HCID 70546801、化合物

実験手順

A solution of 4-methylamino-1-bromo anthraquinone in a solvent such as toluene is heated to reflux for several hours with an excess of 1,3-diamino propane. After the reaction mixture has been treated in a manner similar to that described in Example I, the 4-methylamino-1-(γ-aminopropyl)--amino anthraquinone is isolated and after being crystallized in toluene, melts at 142° C.

後処理

  1. additionAfter the reaction mixture has been treated in a manner similar to

出典と根拠

ORDレコード
ord-f9685d406d404c46a92040ad83d01c99
出典データセット
uspto-grants-1980_10
特許番号
US04226784

関連ノート

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