Diphenyllead dichloride → Diphenyl lead salicylaldehyde

HRID 903105

反応式

HRID 903105 の反応式
[C:1]1([Pb:7](Cl)(Cl)[C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH:16](=[O:24])[C:17]1[C:18](=[CH:20][CH:21]=[CH:22][CH:23]=1)[OH:19].[Na]>CC(C)=O>[CH:16](=[O:24])[C:17]1[C:18](=[CH:20][CH:21]=[CH:22][CH:23]=1)[OH:19].[C:8]1([Pb:7][C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1

参加物

4

反応物 2

HCID 75032Diphenyllead dichlorideHCID 86741752Sodium 2-formylbenzenolate

生成物 1

HCID 88776750Diphenyl lead salicylaldehyde

試薬・触媒・溶媒 1

HCID 180Acetone溶媒

実験手順

Diphenyl lead dichloride (0.01 mol) is mixed with 0.02 mol of sodium salicylaldehyde in acetone. The solution is allowed to stand 10 minutes and then filtered. Water is added to the filtrate to precipitate the lead chelate complex, which is then separated by filtration.

後処理

  1. filtrationfiltered
  2. additionWater is added to the filtrate
  3. customto precipitate the lead chelate complex, which
  4. customis then separated by filtration

出典と根拠

ORDレコード
ord-6ffbe9600a994d89abad6953696604cd
出典データセット
uspto-grants-1980_10
特許番号
US04226792

関連ノート

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