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Ethyl cyano(2,2,6,6-tetramethylpiperidin-4-ylidene)acetate → Cyano(2,2,6,6-tetramethylpiperidin-4-yl)acetic acid, ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl cyano(2,2,6,6-tetramethylpiperidin-4-ylidene)acetate | HCID 712423 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Cyano(2,2,6,6-tetramethylpiperidin-4-yl)acetic acid, ethyl ester | HCID 6420920 | — |
反応手順
This ester is hydrogenated over Pd/C in ethanol and gives ethyl 2-(2,2,6,6-tetramethyl-4-piperidinyl)-cyanoacetate which has a melting point of 116°-117° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04226999 |
| 出典データセット | uspto-grants-1980_10 |
| ORD ID | ord-6768b0ba28304cae8bf3d97b4b9201b2 |
| 出典メモ | uspto-grants-1980_10 |