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HRID 903584作成日:2026年10月26日

Triethylamine → 122570-36-9

https://huagongshe.com/reaction/903584

反応式

関与物質

役割名称HCID仕込み量
反応物TriethylamineHCID 8471—
反応物Dopamine HydrochlorideHCID 65340—
反応物N-acetyl-L-methionineHCID 448580—
溶媒DimethylformamideHCID 6228—
生成物122570-36-9HCID 22812625—

反応手順

2.85 g of dopamine hydrochloride, 4.32 g of N-hydroxysuccinimide ester of N-acetyl-L-methionine, 3.04 g of triethylamine and 15 ml of dimethylformamide are treated in the same manner as described in Example 5. After the reaction, the mixture is condensed under reduced pressure to remove solvent. The residue is dissolve in ethyl acetate, washed with water and dried. The solution is condensed to remove solvent. 3.1 g of N-(N-acetyl-L-methionyl)-dopamine are obtained as caramel.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04228183
出典データセットuspto-grants-1980_10
ORD IDord-6823c088a7c342818f6492ad5f3a1b94
出典メモuspto-grants-1980_10