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Triethylamine → 122570-36-9
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | Dopamine Hydrochloride | HCID 65340 | — |
| 反応物 | N-acetyl-L-methionine | HCID 448580 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 122570-36-9 | HCID 22812625 | — |
反応手順
2.85 g of dopamine hydrochloride, 4.32 g of N-hydroxysuccinimide ester of N-acetyl-L-methionine, 3.04 g of triethylamine and 15 ml of dimethylformamide are treated in the same manner as described in Example 5. After the reaction, the mixture is condensed under reduced pressure to remove solvent. The residue is dissolve in ethyl acetate, washed with water and dried. The solution is condensed to remove solvent. 3.1 g of N-(N-acetyl-L-methionyl)-dopamine are obtained as caramel.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04228183 |
| 出典データセット | uspto-grants-1980_10 |
| ORD ID | ord-6823c088a7c342818f6492ad5f3a1b94 |
| 出典メモ | uspto-grants-1980_10 |