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Methyltryptamine → N-methyl-N-(4-methoxycarbonylbutyryl)-tryptamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyltryptamine | HCID 6088 | — |
| 反応物 | Methyl 4-chloroformylbutyrate | HCID 73916 | — |
| 生成物 | N-methyl-N-(4-methoxycarbonylbutyryl)-tryptamine | HCID 23336480 | 92.9% |
反応手順
10.3 g of N-methyl-tryptamine (i.e., 3-(2-methylaminoethyl)-indole) and 11.7 g of 4-methoxycarbonylbutyryl chloride were treated in the same manner as described in Example 1. 16.6 g of N-methyl-N-(4-methoxycarbonylbutyryl)-tryptamine (i.e., 3-[2-(N-methyl-4-methoxycarbonylbutanamido)ethyl]indole) were therby obtained. Yield: 92.8%
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04228168 |
| 出典データセット | uspto-grants-1980_10 |
| ORD ID | ord-a29b862b14cd4be6ab465ec07efaf95d |
| 出典メモ | uspto-grants-1980_10 |