Diazomethane → HCID 20528716、化合物

HRID 903870ノート

反応式

HRID 903870 の反応式
[C:1]([C:4]1[CH:14]=[CH:13][CH:12]=[C:6]2[C:7]([NH:9][C:10](=[O:11])[C:5]=12)=[O:8])([OH:3])=[O:2].[N+](=[CH2:17])=[N-]>CCOCC>[CH3:17][O:2][C:1]([C:4]1[CH:14]=[CH:13][CH:12]=[C:6]2[C:7]([NH:9][C:10](=[O:11])[C:5]=12)=[O:8])=[O:3]

参加物

4

反応物 2

HCID 9550DiazomethaneHCID 205447191,3-dioxo-2,3-dihydro-1H-isoindole-4-carboxylic acid

生成物 1

HCID 20528716HCID 20528716、化合物

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒2 回

実験手順

To a suspension of 3-carboxyphthalimide (10 g) in ether (50 ml), a solution of diazomethane in ether was added slowly until a faint yellow colouration persisted. Excess of diazomethane was destroyed with acetic acid and the reaction mixture was evaporated to yield the desired compound.

後処理

  1. customExcess of diazomethane was destroyed with acetic acid
  2. customthe reaction mixture was evaporated

出典と根拠

ORDレコード
ord-d285e306ed5e42b19ca3f0039a71a8b7
出典データセット
uspto-grants-1980_10
特許番号
US04229443

反応ノート

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