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HRID 904008作成日:2026年10月26日

Resorcinol → 1,3-Diisopropylbenzene

https://huagongshe.com/reaction/904008

反応式

関与物質

役割名称HCID仕込み量
反応物ResorcinolHCID 5054—
反応物Hydroperoxide,1,1'-[1,3-phenylenebis(1-methylethylidene)]bis-HCID 53471113—
生成物1,3-DiisopropylbenzeneHCID 7450—
生成物m-Diisopropylbenzene monohydroperoxideHCID 71436539—

反応手順

A process for the preparation of resorcin comprising contacting impure meta-diisopropylbenzene dihydroperoxide obtained by liquid phase air oxidation of meta-diisopropylbenzene and/or meta-diisopropylbenzene monohydroperoxide, with a dispersion of a synthetic silica-alumina catalyst having a silica content of 60 to 95% by weight and a specific surface area of at least 100 m2 /g, under refluxing conditions in a mixed solvent of a ketone selected from the group consisting of acetone, methylethylketone and methylisobutyl ketone and an aromatic hydrocarbon selected from the group consisting of benzene, toluene, xylene and ethylbenzene containing 0.3 to 1.0% by weight of water based on the total starting mixture.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04229597
出典データセットuspto-grants-1980_10
ORD IDord-c506e3dcd70942f48cdbbb923e2101a6
出典メモuspto-grants-1980_10