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Timonacic → 3-[4-(4-Pentadecenylamino)benzoyl]-4-carboxythiazolidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Timonacic | HCID 9934 | — |
| 反応物 | 3-[4-(4-Pentadecenylamino)benzoyl]-4-carboethoxythiazolidine | HCID 53653028 | — |
| 溶媒 | Acetone sodium bicarbonate | HCID 86737261 | — |
| 生成物 | 3-[4-(4-Pentadecenylamino)benzoyl]-4-carboxythiazolidine | HCID 53835524 | — |
反応手順
By means of the alkaline hydrolysis method of Example 2 the ethyl ester of Example 385 is converted to the subject carboxylic acid. This acid is also prepared using the procedure of Example 385 except that the acylation of the thiazolidine-4-carboxylic acid is carried out in aqueous acetone sodium bicarbonate solution.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04230878 |
| 出典データセット | uspto-grants-1980_10 |
| ORD ID | ord-a25f4f14ee584281bdb91b5e95b0134e |
| 出典メモ | uspto-grants-1980_10 |