反応式
[CH3:1][CH:2]([CH:6]([CH3:10])[C:7](O)=[O:8])[C:3](O)=[O:4].[NH4+:11].Cl>C(OCC)(=O)C>[CH3:1][CH:2]1[CH:6]([CH3:10])[C:7](=[O:8])[NH:11][C:3]1=[O:4]参加物
5
反応条件
- 温度
- 60 °C
実験手順
1 g of 2,3-dimethylsuccinic acid (a mixture of D-, L-, and meso-isomers) was added to 10 ml of 28% aqueous ammonium solution. The mixture was heated and stirred at about 60° C. for 1 hour. After cooling, to the reaction mixture was added aqueous hydrochloric acid solution so as to neutralize, and then the mixture was extrated twice with 10 ml of ethyl acetate. The extract was concentrated to obtain 0.73 g of 2,3-dimethylsuccinimide (a mixture of D-, L, and meso-isomers).
後処理
- temperatureThe mixture was heated
- temperatureAfter cooling, to the reaction mixture
- concentrationThe extract was concentrated
出典と根拠
- ORDレコード
- ord-64a8af986959487aa0255059ff310410
- 出典データセット
- uspto-grants-1983_12
- 特許番号
- US04419443
関連ノート
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