化工社化工社 化学情報印刷レポート · 研究参考用
Butyl Formate → Dibutyl Oxalate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Butyl Formate | HCID 11614 | — |
| 溶媒 | 1-Butanol | HCID 263 | — |
| 生成物 | Dibutyl Oxalate | HCID 16306 | — |
反応手順
Experiment was run in the same manner as in Example 4 except that the catalyst was replaced by 1.0 wt.% palladium-on-silicon-carbide. As the result, it was found that n-butyl formate was produced in a space time yield of 202 g./l.-catalyst.hr and small amounts of di-n-butyl oxalate and n-butanol were by-produced.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04420633 |
| 出典データセット | uspto-grants-1983_12 |
| ORD ID | ord-57f0fcd15f7c4a6a815b1edb34f42b7d |
| 出典メモ | uspto-grants-1983_12 |