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Fuming sulfuric acid → Sulfuric Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Fuming sulfuric acid | HCID 24681 | — |
| 反応物 | 7-Chloro-2,3-dihydro-4-quinolone | HCID 88974 | — |
| 反応物 | 3-((3-Chlorophenyl)amino)propanoic acid | HCID 12470919 | — |
| 生成物 | Sulfuric Acid | HCID 1118 | — |
| 生成物 | 7-Chloro-2,3-dihydro-4-quinolone | HCID 88974 | — |
反応手順
A process for the preparation of 7-chloro-1,2,3,4-tetrahydroquinolin-4-one which comprises cyclising 3-m-chloroanilinopropionic acid by means of an oleum, then desulphonating the intermediate aromatic sulphonic acids of the formula: ##STR3## (wherein n is 1 or 2) by means of dilute sulphuric acid, and then isolating the 7-chloro-1,2,3,4-tetrahydroquinolin-4-one obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04421918 |
| 出典データセット | uspto-grants-1983_12 |
| ORD ID | ord-a2414c36dbfc4cbcb7a2071797154c4e |
| 出典メモ | uspto-grants-1983_12 |