Dimethylamine → [(4-tert-Butyl-phenyl)-(1-ethyl-2-phenyl-1H-indol-3-yl)-methyl]-dimethyl-amine

HRID 9051

反応式

HRID 9051 の反応式
[CH2:1]([N:3]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[C:4]1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[CH3:2].[Cl-].[C:19]([C:23]1[CH:32]=[CH:31][C:26]([CH:27]=[N+:28]([CH3:30])[CH3:29])=[CH:25][CH:24]=1)([CH3:22])([CH3:21])[CH3:20].C(C1C=CC(C=O)=CC=1)(C)(C)C.CNC>>[C:19]([C:23]1[CH:24]=[CH:25][C:26]([CH:27]([N:28]([CH3:30])[CH3:29])[C:5]2[C:6]3[C:11](=[CH:10][CH:9]=[CH:8][CH:7]=3)[N:3]([CH2:1][CH3:2])[C:4]=2[C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[CH:31][CH:32]=1)([CH3:22])([CH3:20])[CH3:21]

参加物

5

反応物 4

HCID 674DimethylamineHCID 703244-tert-ButylbenzaldehydeHCID 832481-ethyl-2-phenyl-1H-indoleHCID 21985368(4-Tert-butyl-benzylidene)-dimethylammonium chloride

生成物 1

HCID 21985317[(4-tert-Butyl-phenyl)-(1-ethyl-2-phenyl-1H-indol-3-yl)-methyl]-dimethyl-amine

実験手順

The preparation was carried out in accordance with general synthesis instructions 4 from 1-ethyl-2-phenyl-1H-indole and (4-tert-butyl-benzylidene)-dimethylammonium chloride, which had been prepared in accordance with example 44 from 4-tert-butylbenzaldehyde and dimethylamine.

出典と根拠

ORDレコード
ord-599298268d6341939a695a9b3cc6a7f0
出典データセット
uspto-grants-2006_08
特許番号
US07091220B2

関連ノート

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