化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl 3-bromo-2-oxocyclohexanecarboxylate → Ethyl 2-methyl-4,5,6,7-tetrahydrobenzo[d]thiazole-4-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 3-bromo-2-oxocyclohexanecarboxylate | HCID 121765 | — |
| 反応物 | Thioacetamide | HCID 2723949 | — |
| 生成物 | Ethyl 2-methyl-4,5,6,7-tetrahydrobenzo[d]thiazole-4-carboxylate | HCID 12917740 | — |
反応手順
This compound is prepared by action of thioacetamide on 2-bromo-6-carbethoxy-cyclohexanone (II), according to the process described in Example 1. B.p.0.1 =102°-105° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04423056 |
| 出典データセット | uspto-grants-1983_12 |
| ORD ID | ord-08aca623f1f74472b6369945ea3cc76d |
| 出典メモ | uspto-grants-1983_12 |