化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl 3-bromo-2-oxocyclohexanecarboxylate → Ethyl 4,5,6,7-tetrahydro-2-methylbenzothiazole-5-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 3-bromo-2-oxocyclohexanecarboxylate | HCID 121765 | — |
| 反応物 | Thioacetamide | HCID 2723949 | — |
| 生成物 | Ethyl 4,5,6,7-tetrahydro-2-methylbenzothiazole-5-carboxylate | HCID 3018725 | — |
反応手順
The compound is prepared by action of thioacetamide on 2-bromo-5-ethoxycarbonyl cyclohexanone (II), as described in Example 1. B.P.0.4 =116°-120° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04423056 |
| 出典データセット | uspto-grants-1983_12 |
| ORD ID | ord-15e79ab0294346a4b11b26c328310fe4 |
| 出典メモ | uspto-grants-1983_12 |