Carbon Dioxide → HCID 178514403、化合物

HRID 905513

反応式

HRID 905513 の反応式
[N:1]([CH2:10][C:11]([OH:13])=[O:12])([CH2:6][C:7]([OH:9])=[O:8])[CH2:2][C:3]([OH:5])=[O:4].C(=O)(O)O.[NH2:18][NH:19][C:20]([NH2:22])=[NH:21].C(=O)=O>O>[N:1]([CH2:2][C:3]([O-:5])=[O:4])([CH2:6][C:7]([O-:9])=[O:8])[CH2:10][C:11]([O-:13])=[O:12].[NH2:18][NH:19][C:20]([NH2:22])=[NH2+:21].[NH2:18][NH:19][C:20]([NH2:22])=[NH2+:21].[NH2:18][NH:19][C:20]([NH2:22])=[NH2+:21]

参加物

5

反応物 3

HCID 280Carbon DioxideHCID 8758Nitrilotriacetic AcidHCID 178513185HCID 178513185、化合物

生成物 1

HCID 178514403HCID 178514403、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Nitrilotriacetic acid (1.0 g, 5.23 mmol) was dissolved in 10 ml of distilled water. Aminoguanidine bicarbonate (2.14 g, 15.69 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for three days. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as a white solid.

後処理

  1. customThe water was removed in vacuo
  2. temperaturewith heating to approximately 90° C
  3. customThe product was isolated as a white solid

出典と根拠

ORDレコード
ord-3a1b04a135ae49119311cf305d8c8721
出典データセット
uspto-grants-2011_09
特許番号
US08012277B2

関連ノート

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