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3-[(Thiophen-2-ylmethyl)-amino]-phthalic acid dimethyl ester → 3-[(Thiophen-2-ylmethyl)-amino]-phthalic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-[(Thiophen-2-ylmethyl)-amino]-phthalic acid dimethyl ester | HCID 21040138 | — |
| 反応物 | 3-(2-Methoxy-ethylamino)-phthalic acid | HCID 21988519 | — |
| 生成物 | 3-[(Thiophen-2-ylmethyl)-amino]-phthalic acid | HCID 21988596 | — |
反応手順
3-[(Thiophen-2-ylmethyl)-amino]-phthalic acid dimethyl ester (0.88 g, 2.88 mmol) was treated in the same manner as described above for the synthesis 3-(2-methoxy-ethylamino)-phthalic acid. The product of the reaction, which contained a mixture of diacid and monomethyl esters, was used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08012997B2 |
| 出典データセット | uspto-grants-2011_09 |
| ORD ID | ord-0ff03dfa3df742909a41335251af7860 |
| 出典メモ | uspto-grants-2011_09 |