化工社化工社 化学情報印刷レポート · 研究参考用
Ammonium Hydroxide → 2,2-Diethoxyacetamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonium Hydroxide | HCID 14923 | — |
| 反応物 | Ethyl diethoxyacetate | HCID 80169 | — |
| 生成物 | 2,2-Diethoxyacetamide | HCID 100765 | 99% |
反応手順
Ethyl diethoxyacetate (Aldrich) (10 mL, 56.41 mmol) was added to concentrated NH4OH (50 mL) and the mixture allowed to stir until a homogeneous solution was obtained (40 hours). The solvent was then removed under reduced pressure to yield the sub-title compound as fine white needles (8.209 g, 99%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08012967B2 |
| 出典データセット | uspto-grants-2011_09 |
| ORD ID | ord-3c948a6daead4d7a9f915b6f7b70559c |
| 出典メモ | uspto-grants-2011_09 |