Hydrazine → HCID 27055575、化合物
反応式
[CH2:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4][CH2:3][N:2]1[CH2:11][C:12]([O:14]CC)=O.[NH2:17][NH2:18]>C(O)C>[CH2:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4][CH2:3][N:2]1[CH2:11][C:12]([NH:17][NH2:18])=[O:14]参加物
4
実験手順
A solution of 90 (2.0 g, 9.12 mmol) and hydrazine (5.1 g, 91 mmol) in ethanol (30 mL) was heated at reflux overnight. The mixture was concentrated under reduced pressure to give 91 (1.87 g ˜100%) which was used without further purification.
後処理
- temperatureat reflux overnight
- concentrationThe mixture was concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-62c165ed74a74b769d7b88b2dc611239
- 出典データセット
- uspto-grants-2007_09
- 特許番号
- US07265122B2
反応ノート
読み込み中…