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2-Methoxyaniline → 2-Methoxyformanilide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methoxyaniline | HCID 7000 | — |
| 反応物 | 2-Nitroanisole | HCID 7048 | — |
| 触媒 | HCID 178419084 | HCID 178419084 | — |
| 生成物 | 2-Methoxyformanilide | HCID 243581 | 24.8% |
反応手順
The procedure of Example 4 was repeated using o-nitroanisole (4 mmol, 0.55 g) as starting material and vanadium(v) oxide (2.3 mg) instead of sodium molybdate dihydrate. After 2.5 h at 90-95° C. a yield of 24.8% of o-formoanisidide was obtained. o-Anisidine (62.8%) was found to be the main product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07268255B2 |
| 出典データセット | uspto-grants-2007_09 |
| ORD ID | ord-bc26d3108f42421e9d4cda553a606bfd |
| 出典メモ | uspto-grants-2007_09 |