2,5-Dimethyl-3-pyrroline → 4-(2,5-Dimethyl-2,5-dihydropyrrol-1-yl)naphthalene-1-carbonitrile
反応式
[C:1]([C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[C:6](F)=[CH:5][CH:4]=1)#[N:2].[CH3:14][CH:15]1[CH:19]=[CH:18][CH:17]([CH3:20])[NH:16]1>>[CH3:14][CH:15]1[CH:19]=[CH:18][CH:17]([CH3:20])[N:16]1[C:6]1[C:7]2[C:12](=[CH:11][CH:10]=[CH:9][CH:8]=2)[C:3]([C:1]#[N:2])=[CH:4][CH:5]=1参加物
3
実験手順
The title compound (1 mg, 3% yield) was prepared as described for 196MBT2-4 from 1-cyano-4-fluoronaphthalene (20 mg, 0.117 mmol) and 2,5-dimethyl-2,5-dihydro-1H-pyrrole (45 mg, 0.468 mmol).
出典と根拠
- ORDレコード
- ord-91daea77a886464a8eede0658247147b
- 出典データセット
- uspto-grants-2007_09
- 特許番号
- US07268232B2
反応ノート
読み込み中…