化工社化工社 化学情報印刷レポート · 研究参考用
Tetrahydrofuran → Citraconic Acid Hydroxyethyl Methacrylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tetrahydrofuran | HCID 8028 | — |
| 反応物 | 2-Hydroxyethyl Methacrylate | HCID 13360 | — |
| 反応物 | Citraconic acid | HCID 643798 | — |
| 触媒 | Azobisisobutyronitrile | HCID 6547 | — |
| 溶媒 | Diethylethylether | HCID 12430074 | — |
| 生成物 | Citraconic Acid Hydroxyethyl Methacrylate | HCID 86602179 | 96% |
反応手順
To 20 g of tetrahydrofuran (THF) were added 5 g of citraconic acid, 5 g of hydroxyethyl methacrylate and 0.1 g of AIBN. The resulting mixture was reacted at 67° C. for 3 hours, after which, the resulting solution was dropped in diethylethyl ether, thereby obtaining 9.6 g of a photoresist polymer of Formula (IIc).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07270934B2 |
| 出典データセット | uspto-grants-2007_09 |
| ORD ID | ord-bee63e5f9a174a5e828a7e7b25d3b5a0 |
| 出典メモ | uspto-grants-2007_09 |