3-Butyn-2-amine, 2-methyl- → HCID 86607368、化合物

反応式

[Cl:1][C:2]1[CH:3]=[C:4]([CH:19]=[C:20]([Cl:22])[CH:21]=1)[O:5][CH:6]([CH2:16][O:17][CH3:18])[C:7]([NH:9][C:10]([CH3:15])([CH3:14])[C:11]#[C:12]C)=[O:8].NC(C)(C)C#C.NC(C)(C)C#CC>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:19]=[C:20]([Cl:22])[CH:21]=1)[O:5][CH:6]([CH2:16][O:17][CH3:18])[C:7]([NH:9][C:10]([CH3:14])([CH3:15])[C:11]#[CH:12])=[O:8]

参加物

反応物 3

HCID 763193-Butyn-2-amine, 2-methyl-

HCID 114123462-Methylpent-3-yn-2-amine

HCID 69114589HCID 69114589、化合物

生成物 1

HCID 86607368HCID 86607368、化合物

実験手順

2-(3,5-Dichlorophenoxy)-3-methoxy-N-(3-methylbut-1-yn-3-yl)propionamide was prepared in a similar way to 2-(3,5-dichlorophenoxy)-3-methoxy-N-(4-methylpent-2-yn-4-yl)propionamide as described in Example 1 except that 3-amino-3-methylbut-1-yne (commercially available as 90% aqueous solution) was used in place of 4-amino-4-methyl pent-2-yne in Stage 4.

出典と根拠

ORDレコード: ord-3f555933faad48b087c2aa249a019f4c
出典データセット: uspto-grants-2007_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07271130B2

反応ノート

読み込み中…

参加物