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Potassium Carbonate → 1-Amino-2-(3'-methyl-5'-hydroxypentanoxy)-4-hydroxyanthraquinone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 3-Methyl-1,5-pentanediol | HCID 20524 | — |
| 反応物 | Disperse Red 60 | HCID 28531 | — |
| 溶媒 | N-methyl-2-pyrrolidone | HCID 13387 | — |
| 生成物 | 1-Amino-2-(3'-methyl-5'-hydroxypentanoxy)-4-hydroxyanthraquinone | HCID 21524107 | — |
反応手順
12.5 parts of 1-amino-2-phenoxy-4-hydroxyanthraquinone, 13 parts of 3-methyl-1,5-pentanediol, 25 parts of N-methylpyrrolidone, 3 parts of polyethylene oxide of average molecular weight 300 and 2 parts of anhydrous potassium carbonate are stirred for one hour at 150°C under nitrogen. After working up, 10.5 parts of 1-amino-2-(3'-methyl-5'-hydroxypentanoxy)-4-hydroxyanthraquinone are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03968131 |
| 出典データセット | uspto-grants-1976_07 |
| ORD ID | ord-980b59c6845f401095d3ecc891f9df97 |
| 出典メモ | uspto-grants-1976_07 |