(S)-(-)-N-Boc-prolinol → HCID 58984973、化合物
反応式
[C:1]([O:5][C:6]([N:8]1[CH2:14][C@@H:13]([O:15][CH3:16])[CH2:12][C@H:9]1[CH2:10][OH:11])=[O:7])([CH3:4])([CH3:3])[CH3:2].C(OC(N1CCC[C@H]1CO)=O)(C)(C)C>>[C:1]([O:5][C:6]([N:8]1[CH2:14][C@@H:13]([O:15][CH3:16])[CH2:12][C@H:9]1[CH:10]=[O:11])=[O:7])([CH3:4])([CH3:3])[CH3:2]参加物
3
実験手順
With the exception that N-t-butoxycarbonyl-cis-4-methoxy-L-prolinol, instead of N-t-butoxycarbonyl-L-prolinol, was used, the same procedure as in Preparation Example 1-1 was repeated to afford the title compound. 6.94 g (65%).
後処理
- customthe same procedure as in Preparation Example 1-1
出典と根拠
- ORDレコード
- ord-a8efbec2b944404d93bc2a6fc174b1ba
- 出典データセット
- uspto-grants-2016_03
- 特許番号
- US09278996B2
反応ノート
読み込み中…