Adipic Acid → Adipic anhydride
反応式
[CH2:1]([CH2:7][C:8]([OH:10])=[O:9])[CH2:2][CH2:3][C:4]([OH:6])=O>CC(OC(C)=O)=O>[O:10]1[C:4](=[O:6])[CH2:3][CH2:2][CH2:1][CH2:7][C:8]1=[O:9]参加物
3
試薬・触媒・溶媒 1
実験手順
100 g adipinic acid and 100 ml acetanhydride were refluxed for 5 hours. The solvent was removed at a rotovap and 100 ml acetonitrile were added to the residue and the mixture was kept in a freezer over night. Then the mixture was fritted and the resulting residue was washed with 50 ml acetonitrile and dried.
後処理
- customThe solvent was removed at a rotovap and 100 ml acetonitrile
- additionwere added to the residue
- waitthe mixture was kept in a freezer over night
- washthe resulting residue was washed with 50 ml acetonitrile
- customdried
出典と根拠
- ORDレコード
- ord-b2802c144e094899a0ee0c9fa522bb6f
- 出典データセット
- uspto-grants-2016_03
- 特許番号
- US09283186B2
反応ノート
読み込み中…