化工社化工社 化学情報印刷レポート · 研究参考用
Propionic Acid → 3-Fluoro-2,6-dipropyl-4-propionylphenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Propionic Acid | HCID 1032 | — |
| 反応物 | Trifluoromethanesulfonic acid | HCID 62406 | — |
| 反応物 | 3-Fluoro-2,4-dipropylphenol | HCID 21985957 | — |
| 生成物 | 3-Fluoro-2,6-dipropyl-4-propionylphenol | HCID 21985943 | — |
反応手順
Propionic acid (9.07 g, 123 mmol) and 3-fluoro-2,4-dipropylphenol (9.60 g, 49.0 mmol) were mixed in trifluoromethanesulfonic acid (50 mL) as in Example 13, step 1. Purification by chramotography on silica gel using ethyl acetate:hexane (10:90) gave the title compound as a white solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07091230B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-f951ff6e45a44e29983784a13e42f834 |
| 出典メモ | uspto-grants-2006_08 |