(3,4-Dimethoxyphenyl)(pyridin-3-yl)methanol → (3,4-Dimethoxyphenyl)(pyridin-3-yl)methanone

HRID 928757ノート

反応式

HRID 928757 の反応式
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:11]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)[OH:12])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10].CN1C(C(C2C=CC=CN=2)O)=CN=C1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([C:11]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[O:12])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10]

参加物

3

反応物 2

HCID 13475606(3,4-Dimethoxyphenyl)(pyridin-3-yl)methanolHCID 86715604(1-Methyl-1H-imidazol-5-yl)(pyridin-2-yl)methanol

生成物 1

HCID 15077853(3,4-Dimethoxyphenyl)(pyridin-3-yl)methanone

実験手順

The title compound was prepared analogously to the method in Intermediate 25: step b using (3,4-dimethoxyphenyl)(pyridin-3-yl)methanol (Intermediate 27: step a) in place of (1-methyl-1H-imidazol-5-yl)(pyridin-2-yl)methanol.

出典と根拠

ORDレコード
ord-4a3e59f29d7846ae8305512bddb4b711
出典データセット
uspto-grants-2016_03
特許番号
US09290476B2

反応ノート

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