化工社化工社 化学情報印刷レポート · 研究参考用
IN2-(benzyloxycarbonyl)-N6-(tert-butoxycarbonyl)-L-lysine → Z-Lys(boc)-ome
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | IN2-(benzyloxycarbonyl)-N6-(tert-butoxycarbonyl)-L-lysine | HCID 98765 | — |
| 反応物 | Boc-L-Lys(Z)-OMe | HCID 11132998 | — |
| 生成物 | Z-Lys(boc)-ome | HCID 13943124 | — |
反応手順
The title compound was prepared from Z-L-Lys(Boc)OH by following the procedure described for example 4, intermediate 31. Intermediate 49 was characterized by the following spectroscopic data: 1H NMR (DMSO-d6, 300 MHz) δ (ppm) 7.47 (m, 5H), 6.76 (t, 1H), 5.09 (s, 2H), 4.51 (m, 1H), 3.68 (s, 3H), 3.18 (m, 2H), 1.90 (m, 2H), 1.55 (m, 2H), 1.38 (s, 9H), 1.25 (m, 2H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09295732B2 |
| 出典データセット | uspto-grants-2016_03 |
| ORD ID | ord-36658c43afad45e286dcfeca4521230d |
| 出典メモ | uspto-grants-2016_03 |