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4-(Trifluoromethyl)aniline → 4-(4-Trifluoromethylphenylaminosulfonyl)-5-methylisoxazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(Trifluoromethyl)aniline | HCID 9964 | — |
| 反応物 | 5-Methyl-1,2-oxazole-4-sulfonyl chloride | HCID 2776141 | — |
| 反応物 | 2-(4-Trifluoromethylphenylaminosulfonyl)1-ethoxypropene | HCID 56982552 | — |
| 生成物 | 4-(4-Trifluoromethylphenylaminosulfonyl)-5-methylisoxazole | HCID 57089194 | — |
反応手順
AA16 was prepared starting from 2-(4-trifluoromethylphenylaminosulfonyl)1-ethoxypropene under the same conditions as described for AA11. Alternatively, AA16 was prepared from 4-trifluoromethylaniline and 4-chlorosulfonyl-5-methylisoxazole.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05760066 |
| 出典データセット | uspto-grants-1998_06 |
| ORD ID | ord-dc4e9641eb91427b9dcb45310c5bab47 |
| 出典メモ | uspto-grants-1998_06 |