化工社化工社 化学情報印刷レポート · 研究参考用
1,2-Dichlorohexafluorocyclobutane → 1-Chloro 3,3,4,4-tetrafluoro cyclobutene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Dichlorohexafluorocyclobutane | HCID 9643 | — |
| 反応物 | Hexafluorocyclobutene | HCID 12767 | — |
| 生成物 | 1-Chloro 3,3,4,4-tetrafluoro cyclobutene | HCID 12663854 | — |
反応手順
The conversion of 1,2-dichlorohexafluorocyclobutane was 30%, the selectivity of the targeted hexafluorocyclobutene was 96% and a 3.5% selectivity of tetrafluoro-1-chlorocyclobutene was formed as the by-product. The selectivity and the conversion were calculated by multiplying the correction coefficient, which was independently determined by the gas chromatography peak areas. The same procedure was used for the following operations.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05763703 |
| 出典データセット | uspto-grants-1998_06 |
| ORD ID | ord-aba3804530b64007a937b59926300bb1 |
| 出典メモ | uspto-grants-1998_06 |