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化工社化工社 化学情報印刷レポート · 研究参考用
HRID 963913作成日:2026年10月23日

Water → HCID 86752776、化合物

https://huagongshe.com/ja/reaction/963913

反応式

関与物質

役割名称HCID仕込み量
反応物WaterHCID 962—
反応物Butyl Benzyl PhthalateHCID 2347—
反応物AcetylacetoneHCID 31261—
反応物1-(2-Hydroxyethyl)-5-nitro-1H-pyrrole-2-carboxamideHCID 160655—
反応物HCID 178435178HCID 178435178—
溶媒AcetoneHCID 180—
生成物HCID 86752776HCID 86752776—

反応手順

On the first day, 1.31 grams of dispersant, NP-10 (Union Carbide), 1.6 grams of high-resistivity water (very pure water prepared in-house for semiconductor work) and 15 grams of solvent mixture (made from 172 ml acetone and 28 ml acetylacetone) were added and mixed well in a 250 ml polypropylene bottle. Then, 13.0 grams of borosilicate glass powder and 8.75 grams of quartz were added into the mixture and ball milled overnight using 10 mm diameter ZrO2 balls. On the second day, 0.2 gram of binder, Butvar B79 (Monsanto) was added into the mixture and ball milled for one hour. Then 2.41 grams of B79, 2.61 grams of plasticizer, Santicizer 160 (butyl phthalate from Monsanto) were added into the bottle and milled for about 3 hours to obtain a creamy, smooth mixture known as a slip or slurry. The slip was cast on a carrier of Fujimori Mylar™ using a 6 inch wide doctor blade having a 16 mil gap at 14 ft/min at room temperature.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05766528
出典データセットuspto-grants-1998_06
ORD IDord-fc9f3bca285e4359abfa9a73511196ee
出典メモuspto-grants-1998_06